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Flame-Retardant Coating

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Flame-Retardant Coating
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  US008048486B2 (12) Ulllted States Patent (10) Patent N0.: US 8,048,486 B2 Nosker et a]. (45) Date of Patent: Nov. 1, 2011 (54) FLAME-RETARDANT COATING 4,567,096 A 1/1986 Piltingsrud et a1. 4,582,761 A * 4/1986 Liu ............................. .. 428/442 * . (75) Inventors: Thomas Nosker, Stockton, NJ (US); 2 ?gggstrg 1' 524/265 Mark Malar, PiSCaIaWays NJ (Us); 5:977:271 A 11/1999 McKay t a1. Jennifer Lynch, Franklin Park, NJ (US); 6,084,008 A 7/2000 Liu Patrick Nosker, Stockton, N] (Us) 6,106,813 A * 8/2000 Monqlet er a1, ~~~~~~~~~~~~~~~~ ~~ 424/61 6,153,674 A 11/2000 Landin _ . . 6,511,756 B1 1/2003 Obuchi et al. (73) Asslgnee- Rutgers: The state Unlverslty of New 6,528,552 131* 3/2003 lkeguchi et a1, ,,,,,,,,,,,,,, H 522/81 Jersey, New BIHHSWICk, NJ (US) 6,548,157 B2 4/2003 Ghahary 6,706,409 B2* 3/2004 Takano et a1. ............... .. 428/450 ( * ) Notice: Subject to any disclaimer, the term of this 6,849,338 B2 2/2005 Clemens et al~ patent is extended Or adjusted under 35 2001/0046562 A1 11/2001 White?eld et al. 2004/0002559 A1 1/2004 Troutman et a1. U'S'C' 154(b)by Odays' 2004/0025743 A1* 2/2004 Wakizaka t a1. ........ 106/1811 2004/0039098 A1 2/2004 Belmares et al. (21) Appl- NO-I l2l963i709 2004/0097684 A1 * 5/2004 Bruchmann t a1. .......... 528/44 2004/0175407 A1 9/2004 McDaniel (22) Filed; Dec, 9, 2010 2006/0281831 A1 12/2006 Ghahary et a1. (65) Prior Publication Data FOREIGN PATENT DOCUMENTS JP 03081141 A * 4/1991 US 011/0091652 A1 Apr. 21, 2011 JP 08311396 A * 11/1996 Related US. Application Data OTHER UBLICATIONS (60) Division of application NO‘ 11 68 4 5 68 ?led on Mar‘ Gerhart (Thermosetting Acrylic Resins. Industrial and Engineering 9 2007 noW Pat No 7 851 536 which is a Chemistry‘ 1961’ 53(6)’ P‘ 458'459)'* ’ _ ’_ _ ’ ’ _’ _ CAS bstract of CS 39173 AN 9881188518, May 988).* Contlnuatlon-ln-part Of a131311021110n NO- English translation of JP 03081141 (12 pages, Apr. 1991).* PCT/US2006/035861, ?led on Sep. 15, 2006. DerWent Abstract for JP 08311396 (Acc. No. 1997-062036, Nov. . . . . 1996 .* (60) Provlslonal apphcanon NO‘ 60/716,938’ ?led on gel)‘ The Condensed Chemical Dictionary, Tenth Edition, ed. HaWley, p. 15, 2005- 27. (1981). (51) Int CL * cited by examiner C08K /10 2006.01 C08K 3/22 E2006 01; Primary Examiner * ilton 1 Cano ASSI‘SZLU’IZ Examiner i rieann R 52) us. l. ...... .. 427/257; 428/155; 524/436; 524/437; (74) (mm/6y] Age” "r Fm” * OX Rothschlld LLP 106/1826 (57) ABSTRACT (58) Field of Classi?cation Search ....... .. 524/436i437; _ _ _ _ _ 427/257; 428/155; 1061826 A ?ame-retardant coating compos1t1on, Wh1ch 1ncludes a See application ?le for Complete Search history' cross-llnked thermosettlng polymer andametal hydroX1de.A precursor composition for use in preparing the ?ame retar (56) References Cited dant-coating is also presented, Wherein the precursor compo U.S. PATENT DOCUMENTS 3,560,253 A 2/1971 Ashton 4,205,865 A 6/1980 Lange t al. ................ .. 503/206 4,254,177 A * 3/1981 Fulmer 428/3055 4,362,838 A 12/1982 Leep t al. .................. .. 524/444 sition includes a cross-linked therrnosetting polymer Varnish, a metal hydroxide, an alcohol, and ater. A ethod for coat ing an article With a ?ame-retardant coating layer and rticles incorporating the ?ame-retardant coating are also presented. 1 Claim, 7 Drawing Sheets  US. Patent Nov. 1, 2011 Sheet 1 017 US ,048,486 B2 Figure 1.  US. Patent Nov. 1, 2011 Sheet 2 017 US ,048,486 B2 Figure 2.  US. Patent Nov. 1, 2011 Sheet 3 017 US ,048,486 B2 ‘501mm Sim Figure 3.  US. Patent Figure 4. Figure 5. Nov. 1, 2011 US ,048,486 B2 Stabilizing Plate Sample IR Ssnscn‘
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